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HRID2395352

反应详情

EQUATION

反应方程式

HRID 2395352 的结构方程式

REACTANTS

反应物

2
结构：FC(F)(F)c1cc(N=C=S)ccc1Cl
HCID520026

4-Chloro-3-(trifluoromethyl)phenyl isothiocyanate

C8H3ClF3NS

结构：Nc1ccc(Sc2ccc(-c3ccccc3)nn2)cc1
HCID18971661

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)(F)c1cc(NC(=S)Nc2ccc(Sc3ccc(-c4ccccc4)nn3)cc2)ccc1Cl
HCID18971682

未命名化合物

收率 69.1%

PROCEDURE

实验过程

3-(4-aminophenylthio)-6-phenylpyridazine (7.0 mmoles, 2.0 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (7.0 mmoles, 1.66 g) were reacted according to procedure C to yield of the title compound 2.5 g, 69%. Mass Spec (FD) 516. Calculated for C24H16ClF3 N4O2S2 : C, 55.76; H, 3.12; N, 10.84. Found: C, 55.98 H, 3.19; N, 10.78.