HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetaldehyde → HCID 18971828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetaldehyde | HCID 33 | — |
| Reactant | HCID 18971770 | HCID 18971770 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18971828 | HCID 18971828 | 63.2% |
Reaction Steps
A solution of 130 mg of 3-cyclopentyloxy-4-methoxybenzthioamide and 100 mg of chloroacetaldehyde in 15 ml of ethanol was heated at reflux for 6 hours. The volatiles were evaporated and the residue purified on silica gel with CH2Cl2 to give 90 mg of product. M.P.: 72°-75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05814651 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-dbc5468491db4b0e9cf0ec5b8f20af6c |
| Source note | uspto-grants-1998_09 |