HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 53989599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | HCID 18989161 | HCID 18989161 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53989599 | HCID 53989599 | — |
Reaction Steps
A mixture of 5-(3-cyclopropyl-1,3-dioxoprop-1-yl)-3,4-dimethoxybenzo[b]thiophene (0.5 g) and triethyl orthoformate (0.73 g) was heated under reflux with acetic anhydride (10 ml) for 3 hours. After cooling and addition of toluene the solution was evaporated to dryness to yield 5-(3-cyclopropyl-2-ethoxymethylene-1,3-dioxoprop-1-yl)-3,4-dimethoxybenzo[b]thiophene as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05489570 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-55d2b7b19e4f43e5a757797d6c2bd339 |
| Source note | uspto-grants-1996_02 |