HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54421939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18989445 | HCID 18989445 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54421939 | HCID 54421939 | — |
Reaction Steps
334 ml of concentrated HCl are added over 10 minutes to a solution of 404.5 g (1.84 mol) of α-ethenyl-2-fluoro-3-(trifluoromethyl)benzenemethanol (prepared according to Example I1) in 3.7 1 of dioxane and the mixture is then heated for 2 h at reflux. 83.5 ml of concentrated HCl are added and the mixture is heated for a further 2 h at reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05489592 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-bd32231425bc4ed99f329d736c1e1016 |
| Source note | uspto-grants-1996_02 |