Azobisisobutyronitrile → HCID 53984011, compound

Participants

Reaction Steps

A mixture of 4.3 g (0.02 mol) of 5-bromo-2-fluoro-1-(1-propenyl) benzene, 100 ml of carbon tetrachloride, 0.07 g of azobisisobutyronitrile and 3.6 g (0.02 mol) of N-bromosuccinimide is heated for 5 h at reflux. The solid is filtered, the filtrate is evaporated under vacuum and the residue used without other purification in the following stage: Yd.: 5.4 g (91%)

Provenance & Evidence