Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 4-Aminobenzoic acid hydrazide | HCID 21450 | — |
| Reactant | HCID 21933416 | HCID 21933416 | — |
| Product | HCID 15292877 | HCID 15292877 | — |
Reaction Steps
A mixture of 4.5 g (29.8 mmol) of 4-aminobenzoic acid hydrazide and 2.6 mL of ethylthioisocyanate in 15 mL of acetonitrile was heated at reflux for 3 hours. The solution was cooled to 24° C., and the precipitate was collected by filtration and dried under vacuum to afford 7.0 g of 1-(4-aminobenzoyl)-4-ethylthiosemicarbazide, mp 113°-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05489598 |
|---|
| Source dataset | uspto-grants-1996_02 |
|---|
| ORD ID | ord-754bd0cffe3f4ff7a14ced059730769f |
|---|
| Source note | uspto-grants-1996_02 |
|---|
