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HRID2395773

反应详情

EQUATION

反应方程式

HRID 2395773 的结构方程式

REACTANTS

反应物

2
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：COC(=O)c1cc2ccc(N(C)C)cc2[nH]1
HCID4715276

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1ccc2cc(C(=O)O)[nH]c2c1
HCID5159908

6-Dimethylamino-1H-indole-2-carboxylic acid

C11H12N2O2

PROCEDURE

实验过程

Following the general procedure of PREPARATION 63 and making non-critical variations but starting with methyl 6-(N,N-dimethylamino)indole-2-carboxylate (PREPARATION 88, 0.80 g), potassium hydroxide (0.25 g), the title compound is obtained, NMR (300 MHz, CD3OD) 7.62, 7.13, 7.11, 7.01, and 3.11 δ.

WORKUP

后处理

  1. customthe general procedure of PREPARATION 63