HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 6-(dimethylamino)-1H-indole-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | methyl 6-(dimethylamino)-1H-indole-2-carboxylate | HCID 4715276 | — |
| Product | 6-(dimethylamino)-1H-indole-2-carboxylic acid | HCID 5159908 | — |
Reaction Steps
Following the general procedure of PREPARATION 63 and making non-critical variations but starting with methyl 6-(N,N-dimethylamino)indole-2-carboxylate (PREPARATION 88, 0.80 g), potassium hydroxide (0.25 g), the title compound is obtained, NMR (300 MHz, CD3OD) 7.62, 7.13, 7.11, 7.01, and 3.11 δ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05489593 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-2a2183cb021549fb8816cb1dc407b928 |
| Source note | uspto-grants-1996_02 |