HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexahydro-1,4-diazepine → HCID 21477605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexahydro-1,4-diazepine | HCID 68163 | — |
| Reactant | 3-Chloro-N-(propan-2-yl)pyrazin-2-amine | HCID 21477637 | — |
| Product | HCID 21477605 | HCID 21477605 | — |
Reaction Steps
Following the general procedure of PREPARATION 24 and making non-critical variations but starting with homopiperazine (2.46 g) and 2-chloro-3-(1-methylethyl)aminopyrazine (PREPARATION 23), the title compound is obtained, NMR (300 MHz, CDCl3) 7.56, 7.34, 4.75, 4.04, 3.28-3.18, 3.00-2.94, 1.79, and 1.15 δ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05489593 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-5400d8a8aec842c7b5642e8374c7a5b7 |
| Source note | uspto-grants-1996_02 |