HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15230315, compound → HCID 15230316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15230315 | HCID 15230315 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 15230316 | HCID 15230316 | 99% |
Reaction Steps
A solution of 0.80 g (1.45 mmole) of the nitrobenzene derivative of Example 43 in 50% methanol-THF is reduced with 5% palladium-on-carbon catalyst. The filtered solution is concentrated at reduced pressure to give 0.75 g of pure product as a solid foam; mass spectrum (EI) 522 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05489686 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-dce3b468351046569dec995f931dcdec |
| Source note | uspto-grants-1996_02 |