Trifluoroacetic acid → HCID 178525683, compound

HRID 2396023Notes

Reaction equation

[B:1](Br)(Br)Br.[F:5][C:6]([F:11])([F:10])[C:7]([OH:9])=[O:8]>>[F:5][C:6]([F:11])([F:10])[C:7]([O-:9])=[O:8].[F:5][C:6]([F:11])([F:10])[C:7]([O-:9])=[O:8].[F:5][C:6]([F:11])([F:10])[C:7]([O-:9])=[O:8].[B+3:1]

Participants

Reactant 2

HCID 6422Trifluoroacetic acid

HCID 25134Boron tribromide

Product 1

HCID 178525683HCID 178525683, compound

Procedure

Place boron tribromide (215 mg, 0.86 mmol) in a flask and cool to 0°C. Cautiously add trifluoroacetic acid (5 mL) with stirring. Evaporate the solvent to give boron tris(trifluoroacetate).

Workup

customEvaporate the solvent

Sources & evidence

ORD record: ord-8a01327e6a124f15939d30e1d956c560
Source dataset: uspto-grants-1996_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05491143

Reaction notes

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