反应详情

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

1. temperatureunder reflux for 20 hours
2. temperatureThe reaction mixture was cooled
3. customthe excess ethanol was removed under vacuum