Diisopropylaniline → N-(2,6-Diisopropyl-phenyl)-2-(2,6-diisopropyl-phenylsulfamoyl)-acetamide

HRID 2396095Notes

Reaction equation

[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[NH:13][S:14]([CH2:17][C:18]([NH:20]C1N=NN(CCCCCCCCCCCC)N=1)=[O:19])(=[O:16])=[O:15])([CH3:3])[CH3:2].[CH:38]([C:41]1[CH:47]=[CH:46][CH:45]=[C:44]([CH:48]([CH3:50])[CH3:49])[C:42]=1N)([CH3:40])[CH3:39]>>[CH:48]([C:44]1[CH:45]=[CH:46][CH:47]=[C:41]([CH:38]([CH3:40])[CH3:39])[C:42]=1[NH:20][C:18](=[O:19])[CH2:17][S:14](=[O:16])(=[O:15])[NH:13][C:5]1[C:6]([CH:10]([CH3:11])[CH3:12])=[CH:7][CH:8]=[CH:9][C:4]=1[CH:1]([CH3:3])[CH3:2])([CH3:50])[CH3:49]

Participants

Reactant 2

HCID 32484Diisopropylaniline

HCID 189886562-(2,6-Diisopropyl-phenylsulfamoyl)-N-(dodecyl-2-H-tetrazol-5-yl)-acetamide

Product 1

HCID 15341055N-(2,6-Diisopropyl-phenyl)-2-(2,6-diisopropyl-phenylsulfamoyl)-acetamide

Procedure

This compound was prepared in the same manner as for the title compound of Example 2, except that 2-DAT was replaced with 2,6-diisopropylaniline, mp 202°-205° C.

Sources & evidence

ORD record: ord-d687ef1f0a4641c1bd81578e1f7b1ee0
Source dataset: uspto-grants-1996_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05491170

Reaction notes

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