1-Dodecanethiol → HCID 15341061, compound

HRID 2396106Notes

Reaction equation

HRID 2396106 reaction equation
C(C1C=CC=C(C(C)C)C=1N[S:14]([CH2:17][C:18](NC1N=NN(CCCCCCCCCCCC)N=1)=[O:19])(=[O:16])=[O:15])(C)C.C(C1C=CC=C(C(C)C)C=1N)(C)C.[O:51]([C:55]1[CH:61]=[C:60]([O:62][CH:63](C)C)[CH:59]=[C:58]([O:66][CH:67](C)C)[C:56]=1[NH2:57])[CH:52](C)C.[CH2:70]([SH:82])[CH2:71][CH2:72][CH2:73][CH2:74][CH2:75][CH2:76][CH2:77][CH2:78][CH2:79][CH2:80][CH3:81]>>[CH2:70]([S:82][C:18](=[O:19])[CH2:17][S:14](=[O:16])(=[O:15])[NH:57][C:56]1[C:58]([O:66][CH3:67])=[CH:59][C:60]([O:62][CH3:63])=[CH:61][C:55]=1[O:51][CH3:52])[CH2:71][CH2:72][CH2:73][CH2:74][CH2:75][CH2:76][CH2:77][CH2:78][CH2:79][CH2:80][CH3:81]

Participants

5

Reactant 4

HCID 81951-DodecanethiolHCID 32484DiisopropylanilineHCID 189886562-(2,6-Diisopropyl-phenylsulfamoyl)-N-(dodecyl-2-H-tetrazol-5-yl)-acetamideHCID 18988666HCID 18988666, compound

Product 1

HCID 15341061HCID 15341061, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 2, except that 2,6-diisopropylaniline was replaced with 2,4,6-triisopropoxylaniline and 2-DAT was replaced with dodecanthiol, mp 90°-93° C.

Sources & evidence

ORD record
ord-ede87de20fe84304ad705293cb40d434
Source dataset
uspto-grants-1996_02
Patent number
US05491170

Reaction notes

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