HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70042532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22858686 | HCID 22858686 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70042532 | HCID 70042532 | — |
Reaction Steps
N-[N-[2-(N-tert-Butoxycarbonyl-N-methylamino)ethyl]-N-methylaminocarbonyl]-L-phenylalanine benzyl ester (11 g was dissolved in a solution of 4M hydrogen chloride in ethyl acetate (200 ml) under ice-bath cooling. After being stirred at the same temperature for 30 minutes, the solution was concentrated in vacuo to give N-[N-[2-(N-methylamino)ethyl]-N-methylaminocarbonyl]-L-phenylalanine benzyl ester hydrochloride (10 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491132 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-1a2b3f4b29c94b819b219ee4635205a3 |
| Source note | uspto-grants-1996_02 |