Decanoyl chloride → Sulfamic acid (decanoyl)-2,6-bis(1-methylethyl)phenyl ester

HRID 2396264Notes

Reaction equation

CC([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10](C)[CH3:11])[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.C(C1C=CC=C(C(C)C)C=1CC(Cl)=O)(C)C.C(Cl)(=O)CCCCCCCCC>>[C:14]([C:16]1[C:17]([CH:30]([CH3:31])[CH3:32])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][CH:21]=1)(=[O:15])[CH2:13][CH2:5][CH2:4][CH2:9][CH2:8][CH2:7][CH2:6][CH2:10][CH3:11]

Participants

Reactant 3

HCID 66982Decanoyl chloride

HCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl ester

HCID 193627822,6-Diisopropylphenylacetyl chloride

Product 1

HCID 10201701Sulfamic acid (decanoyl)-2,6-bis(1-methylethyl)phenyl ester

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetyl chloride was replaced with decanoyl chloride, mp 92°-94° C.

Sources & evidence

ORD record: ord-880fcd22731143e79bb573483a8bb340
Source dataset: uspto-grants-1996_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05491172

Reaction notes

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