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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396488Generated: October 30, 2026

HCID 10825133, compound → HCID 10559045, compound

https://huagongshe.com/reaction/2396488

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10825133HCID 10825133—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 10559045HCID 10559045—

Reaction Conditions

Temperature45 °C

Reaction Steps

5.8 g of the compound obtained in Step b, in 30 ml of absolute ethanol, and 100 mg of 10% palladium-on-carbon are stirred and heated at 45° C. under a hydrogen atmosphere for 3 hours. The solvent is evaporated off. After customary treatment of the organic phase, the desired crude product is purified by distillation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05492912
Source datasetuspto-grants-1996_02
ORD IDord-31a2d50cd43f4986bc071197bce7fb63
Source noteuspto-grants-1996_02