Catechol → HCID 18987817, compound

HRID 2396603Notes

Reaction equation

HRID 2396603 reaction equation
[B:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][N:11]2[C:15]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:14]([S:21][CH3:22])[N:13]=[C:12]2[CH2:23][CH2:24][CH2:25][CH3:26])=[CH:6][CH:5]=1)([OH:3])[OH:2].[C:27]1([C:29](=[CH:31][CH:32]=[CH:33][CH:34]=1)O)O>>[CH2:23]([C:12]1[N:11]([CH2:10][C:7]2[CH:8]=[CH:9][C:4]([B:1]3[O:2][C:34]4[CH:33]=[CH:32][CH:31]=[CH:29][C:27]=4[O:3]3)=[CH:5][CH:6]=2)[C:15]([C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:14]([S:21][CH3:22])[N:13]=1)[CH2:24][CH2:25][CH3:26]

Participants

3

Reactant 2

HCID 289CatecholHCID 18400107HCID 18400107, compound

Product 1

HCID 18987817HCID 18987817, compound

Procedure

Using the procedure of Preparation 4, 1 g of ethyl 1-[(4-boronophenyl)-methyl]-2-butyl-4-(methylthio)-1H-imidazole-5-carboxylate and 0.293 g of catechol were reacted to obtain the desired product.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-d2c767905fc141e49e5e3c2068f7f561
Source dataset
uspto-grants-1996_02
Patent number
US05493046

Reaction notes

Loading…