HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → N~1~,N~1~,N~2~,N~2~-Tetrakis(3-methylphenyl)benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 3-Iodotoluene | HCID 12268 | — |
| Product | N~1~,N~1~,N~2~,N~2~-Tetrakis(3-methylphenyl)benzene-1,2-diamine | HCID 18985805 | — |
Reaction Steps
The procedure of Example 1 was repeated except the use of 5.4 g of o-phenylenediamine of the formula (12) and 42.6 g of m-iodotoluene of the formula (14): ##STR11## as a starting material to obtain the expected compound of the formula (4) (12.6 g, yield: 55.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05494765 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-736041858eb54ca8a1d2a9b255171609 |
| Source note | uspto-grants-1996_02 |