HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 56985223, compound → HCID 57220130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 56985223 | HCID 56985223 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57220130 | HCID 57220130 | — |
Reaction Steps
This compound was prepared in analogy to Example 1g) starting from t-butyl (1S,4R, 5R)-6-(3,4-dimethoxybenzyl)-7-oxo-4-[2-oxo-3-(2-trimethylsilanyl-ethoxy)-propyl]-2,6-diazabicyclo[3.2.0]heptane-2-carboxylate (25.7 g; 48 mmol). Yield: 12.7 g (69%) as a colourless solid. M.p. 89°-91° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05494666 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-5a6462db6fd0450baacf671180b99fe6 |
| Source note | uspto-grants-1996_02 |