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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396671Generated: October 30, 2026

HCID 56985223, compound → HCID 57220130, compound

https://huagongshe.com/reaction/2396671

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 56985223HCID 56985223—
SolventEthyl AcetateHCID 8857—
ProductHCID 57220130HCID 57220130—

Reaction Steps

This compound was prepared in analogy to Example 1g) starting from t-butyl (1S,4R, 5R)-6-(3,4-dimethoxybenzyl)-7-oxo-4-[2-oxo-3-(2-trimethylsilanyl-ethoxy)-propyl]-2,6-diazabicyclo[3.2.0]heptane-2-carboxylate (25.7 g; 48 mmol). Yield: 12.7 g (69%) as a colourless solid. M.p. 89°-91° C. (ethyl acetate).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05494666
Source datasetuspto-grants-1996_02
ORD IDord-5a6462db6fd0450baacf671180b99fe6
Source noteuspto-grants-1996_02