HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 18986570, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 15294772 | HCID 15294772 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18986570 | HCID 18986570 | — |
Reaction Steps
A mixture of 4.1 g of 1-(2-(tetralin-1-yl)ethyl)-4-(3,4-dimethoxyphenyl)piperidine (fumarate, m.p. 154°-156°) 3.2 g of pyridine hydrochloride and 80 ml of pyridine is boiled for 3 hours. It is cooled, evaporated and worked up in the customary manner and gives 1-(2-(tetralin-1-yl)ethyl)-4-(3,4-dihydroxyphenyl)piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05495022 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-d3fd54b63f394ce6a5170eb2fd5c451b |
| Source note | uspto-grants-1996_02 |