HRID2396883

反应详情

EQUATION

反应方程式

HRID 2396883 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of 3.2 g of 1-(2-(6-nitrotetralin-1-yl)ethyl)-4-(3,4-dimethoxyphenyl)piperidine in 50 ml of methanol is hydrogenated in the presence of 1.6 g of Pd/C (5%) until the absorption of hydrogen has come to a standstill. The catalyst is filtered off, and the filtrate is worked up in the customary manner and gives 1-(2-(6-aminotetralin-1-yl) ethyl)-4-(3,4-dimethoxyphenyl)piperidine.

WORKUP

后处理

  1. customis hydrogenated in the presence of 1.6 g of Pd/C (5%) until the absorption of hydrogen
  2. filtrationThe catalyst is filtered off