HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-ethyl-2-hydroxyimino-5-nitro-3-hexen-1-yl)-3-pyridinecarboxamide → HCID 53837090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-ethyl-2-hydroxyimino-5-nitro-3-hexen-1-yl)-3-pyridinecarboxamide | HCID 4532 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 53837090 | HCID 53837090 | — |
Reaction Steps
A mixture of N-(4-ethyl-2-hydroxyimino-5-nitro-3-hexen-1-yl)-3-pyridinecarboxamide (306 mg), 3-chloroperbenzoic acid (323 mg), chloroform (15 ml) and acetone (40 ml) was stirred at room temperature for 10 hours. The resulting precipitates were collected and washed with acetone to give N-(4-ethyl-2-hydroxyimino-5-nitro-3-hexen-1-yl)-3-pyridinecarboxamide 1-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05495023 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-19655a1247d74b8ba6be2d9fb62e4be5 |
| Source note | uspto-grants-1996_02 |