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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396934Generated: October 29, 2026

Acetic Acid → HCID 18986670, compound

https://huagongshe.com/reaction/2396934

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantO-CresolHCID 335—
ReactantFormaldehydeHCID 712—
ReactantDibutylamineHCID 8148—
ReactantMethallyl alcoholHCID 10557—
ProductHCID 18986670HCID 18986670—

Reaction Conditions

Temperature170 °C

Reaction Steps

A pressure-proof reaction vessel equipped with a stirrer was charged with 16.2 g (0.15 mole) of o-cresol, 54.1 g (0.75 mole) of 2-methyl-2-propen-1 -ol, 6.2 g (0.165 mole) of 80% paraformaldehyde, 1.9 g (0.01 5 mole) of dibutylamine and 4.5 g (0.075 mole) of acetic acid, and the mixture was reacted, with stirring, at 170° C. for 6 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05495026
Source datasetuspto-grants-1996_02
ORD IDord-3bdd066daa8241dba580bb12fe9aec4a
Source noteuspto-grants-1996_02