Acetic Acid → HCID 18986670, compound

HRID 2396934Notes

Reaction equation

HRID 2396934 reaction equation
[C:1]1([CH3:8])[C:6]([OH:7])=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:9][C:10](=[CH2:13])[CH2:11][OH:12].C=O.[CH2:16](NCCCC)CCC.C(O)(=O)C>>[CH3:13][C:10]1([CH2:11][OH:12])[CH2:9][CH2:16][C:5]2[C:6](=[C:1]([CH3:8])[CH:2]=[CH:3][CH:4]=2)[O:7]1

Participants

6

Reactant 5

HCID 176Acetic AcidHCID 335O-CresolHCID 712FormaldehydeHCID 8148DibutylamineHCID 10557Methallyl alcohol

Product 1

HCID 18986670HCID 18986670, compound

Conditions

Temperature
170 °C

Procedure

A pressure-proof reaction vessel equipped with a stirrer was charged with 16.2 g (0.15 mole) of o-cresol, 54.1 g (0.75 mole) of 2-methyl-2-propen-1 -ol, 6.2 g (0.165 mole) of 80% paraformaldehyde, 1.9 g (0.01 5 mole) of dibutylamine and 4.5 g (0.075 mole) of acetic acid, and the mixture was reacted, with stirring, at 170° C. for 6 hours.

Workup

  1. customA pressure-proof reaction vessel
  2. customequipped with a stirrer
  3. customthe mixture was reacted

Sources & evidence

ORD record
ord-3bdd066daa8241dba580bb12fe9aec4a
Source dataset
uspto-grants-1996_02
Patent number
US05495026

Reaction notes

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