4-Nitrobenzenesulfonyl fluoride → HCID 178506412, compound

HRID 2397133Notes

Reaction equation

HRID 2397133 reaction equation
O=[N+]([O-])c1ccc(S(=O)(=O)F)cc1.O[C@H]1C[C@@H](OCc2ccccc2)C1>C1CCOC1.CC(C)(C)N=P(N1CCCC1)(N1CCCC1)N1CCCC1>F[C@H]1C[C@@H](OCc2ccccc2)C1

Participants

5

Reactant 2

HCID 1882464-Nitrobenzenesulfonyl fluorideHCID 178521639HCID 178521639, compound

Product 1

HCID 178506412HCID 178506412, compoundYield 22%

Reagents, catalysts & solvents 2

HCID 3856267tert-Butylimino-tri(pyrrolidino)phosphoraneReagentHCID 8028TetrahydrofuranSolvent2×

Workup

  1. additionNo procedure recorded

Sources & evidence

ORD record
ord-e6373b9b3ff04773bd0668868f65357f
Source dataset
Deoxyfluorination screen
Original link
View source

Reaction notes

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