HRID2397305

反应详情

EQUATION

反应方程式

HRID 2397305 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ethyl N-(4-ethoxycarbonylphenyl)formimidate (Example Ia) (6.6 g, 0.03 mol) and N-octylaniline (6.2 g, 0.03 mol) were heated at 180° until 1.7 ml of ethanol had been collected by distillation. The resulting pale yellow oil was flash distilled to yield the desired product, bp≈235° C. (0.05 mm). ##STR15##

WORKUP

后处理

  1. distillationhad been collected by distillation
  2. distillationdistilled