HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20038059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 21437839 | HCID 21437839 | — |
| Product | HCID 20038059 | HCID 20038059 | — |
Reaction Steps
A mixture of ethyl N-(3-hydroxy-4-methoxycarbonylphenyl)formimidate (6.6 g, 0.03 mol) and N-methylaniline (3.2 g, 0.03 mol) were heated at 150° until 1.7 mol of ethanol had been collected by distillation. The pale yellow oil was flash distilled to yield the desired product, bp≈200° C. (0.1 mm). ##STR16##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021471 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-3f38ad06c9a6441b8976e8ab8087ef60 |
| Source note | uspto-grants-1977_05 |