HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 21437957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 21437918 | HCID 21437918 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 21437957 | HCID 21437957 | 84% |
Reaction Steps
Prepared analogous to Example 1 from 4-(2'-chloro-4'-fluoro-4-biphenylyl)-4-oxo-butyric acid. Yield: 84% of theory; m.p. 81°-82° C. (petroleum ether-cyclohexane). Melting point of the cyclohexylamine salt: 148°-149° C. (from ethyl acetate/methanol 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-d03cf958fdc542b49f9004433fa2b166 |
| Source note | uspto-grants-1977_05 |