HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → 4-(3',4'-Dichloro-4-biphenylyl)-butyric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-(3',4'-Dichloro-4-biphenylyl)-4-oxo-butyric acid | HCID 18364134 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 4-(3',4'-Dichloro-4-biphenylyl)-butyric acid | HCID 21437935 | 62% |
Reaction Steps
Prepared analogous to Example 1 from 4-(3',4'-dichloro-4-biphenylyl)-4-oxo-butyric acid. Yield: 62% of theory. Melting point of the cyclohexylamine salt: 167°-168° C. (from isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-dbdba719b760422a9c96a563df749ce8 |
| Source note | uspto-grants-1977_05 |