HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → 4-(4'-Chloro-2'-methyl-4-biphenylyl)-butyric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-(4'-Chloro-2'-methyl-4-biphenylyl)-4-oxo-butyric acid | HCID 21437970 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(4'-Chloro-2'-methyl-4-biphenylyl)-butyric acid | HCID 21437966 | 76% |
Reaction Steps
Prepared analogous to Example 1 by reduction of 4-(4'-chloro-2'-methyl-4-biphenylyl)-4-oxo-butyric acid. Yield: 76%. Melting point of the cyclohexylamine salt: 145.5°-147° C. (from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-4d5f13f088e94ec89b4b484caa0dc068 |
| Source note | uspto-grants-1977_05 |