HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 21437914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-(2'-Fluoro-4'-chloro-4-biphenylyl)-4-oxo-butyric acid | HCID 18364124 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 21437914 | HCID 21437914 | 69% |
Reaction Steps
Prepared analogous to Example 25 from 4-(2'-fluoro-4'-chloro-4-biphenylyl)-4-oxo-butyric acid. Yield: 69% of theory; m.p. of the cyclohexylamine salt: 165°-167° C. (from isopropanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-e9e17355efed46dbb1bcd0a03d1b52df |
| Source note | uspto-grants-1977_05 |