Cyclohexylamine → HCID 21437971, compound

HRID 2397400Notes

Reaction equation

HRID 2397400 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([C:14](=[O:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[C:4]([N+:21]([O-:23])=[O:22])[CH:3]=1.C1(N)CCCCC1>C(O)(C)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([CH:14]([OH:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[C:4]([N+:21]([O-:23])=[O:22])[CH:3]=1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 21437937HCID 21437937, compound

Product 1

HCID 21437971HCID 21437971, compoundYield 46%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Prepared analogous to Example 25 from 4-(4'-chloro-2'-nitro-4-biphenylyl)-4-oxo-butyric acid. Yield: 46% of theory. Melting point of the cyclohexylamine salt: 171°-172° C. (from isopropanol).

Sources & evidence

ORD record
ord-425e378cef3043cc96a15ae1f99a5192
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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