Cyclohexylamine → HCID 21437952, compound

HRID 2397401Notes

Reaction equation

HRID 2397401 reaction equation
[N+:1]([C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:5]=1[C:11]1[CH:16]=[CH:15][C:14]([C:17](=[O:23])[CH2:18][CH2:19][C:20]([OH:22])=[O:21])=[CH:13][CH:12]=1)([O-:3])=[O:2].C1(N)CCCCC1>C(O)(C)C>[N+:1]([C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:5]=1[C:11]1[CH:16]=[CH:15][C:14]([CH:17]([OH:23])[CH2:18][CH2:19][C:20]([OH:22])=[O:21])=[CH:13][CH:12]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 21437962HCID 21437962, compound

Product 1

HCID 21437952HCID 21437952, compoundYield 68%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Prepared analogous to Example 25 from 4-(2'-nitro-4'-methyl-4-biphenylyl)-4-oxo-butyric acid. Yield: 68% of theory. Melting point of the cyclohexylamine salt: 156°-157° C. (from isopropanol).

Sources & evidence

ORD record
ord-d43c3fbaa0584097816a4266cd15b31c
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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