HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21437931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 21437981 | HCID 21437981 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21437931 | HCID 21437931 | 44% |
Reaction Steps
Prepared analogous to Example 46 from the morpholine salt of 4-(3',4'-difluoro-4-biphenylyl)-4-hydroxy-crotonic acid in methanol. Melting point of the cyclohexylamine salt: 170°-171° C. (from water). Yield: 44% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-180983b024eb4c4fb2ae03b04c68ee35 |
| Source note | uspto-grants-1977_05 |