HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21437948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 21437979 | HCID 21437979 | — |
| Product | HCID 21437948 | HCID 21437948 | 94% |
Reaction Steps
Prepared analogous to Example 25 from 4-(2'-cyanobiphenylyl)-4-oxo-butyric acid. Melting point of the cyclohexylamine salt: 167°-168° C. (from ethyl acetate by addition of 15% methanol). Yield: 94% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-ae6108f7a16244d9a88182783a1febe6 |
| Source note | uspto-grants-1977_05 |