HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 21437961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 3′-Chloro-γ-oxo[1,1′-biphenyl]-4-butanoic acid | HCID 23005237 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21437961 | HCID 21437961 | 65% |
Reaction Steps
Prepared analogous to Example 25 from 4-(3'-chloro-4-biphenylyl)-4-oxo-butyric acid. Melting point of the cyclohexylamine salt: 160°-161° C. (from ethyl acetate by addition of methanol). Yield: 65% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021479 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-55c3bd4b006e46339b7dcb3bd8e6eb76 |
| Source note | uspto-grants-1977_05 |