HRID2397425
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Magnesium β-alaninate was prepared by reacting 3.6 g. of β-alanine with 1.8 g. of basic magnesium carbonate in 40 g. of water, while agitating at 75° C. for one half hour. To the cooled slurry was added 2.5 g. of sodium tartrate. After five minutes of stirring, 80 g. of zirconyl hydroxychloride solution (14.4% Zr) was added to the above slurry with agitation. The solution cleared on stirring and had a final pH of 3.3. The product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg and found to contain 33.1% Zr, 1.3% Mg, 1.4% Na, and 10.3% β-alanine.
WORKUP
后处理
- additionTo the cooled slurry was added 2.5 g
- stirringon stirring
- customThe product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg