HRID2397425

反应详情

EQUATION

反应方程式

HRID 2397425 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Magnesium β-alaninate was prepared by reacting 3.6 g. of β-alanine with 1.8 g. of basic magnesium carbonate in 40 g. of water, while agitating at 75° C. for one half hour. To the cooled slurry was added 2.5 g. of sodium tartrate. After five minutes of stirring, 80 g. of zirconyl hydroxychloride solution (14.4% Zr) was added to the above slurry with agitation. The solution cleared on stirring and had a final pH of 3.3. The product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg and found to contain 33.1% Zr, 1.3% Mg, 1.4% Na, and 10.3% β-alanine.

WORKUP

后处理

  1. additionTo the cooled slurry was added 2.5 g
  2. stirringon stirring
  3. customThe product was oven-dried at 55° C. under a vacuum of 40 cm. of Hg