HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 21435859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 21435857 | HCID 21435857 | — |
| Product | HCID 21435859 | HCID 21435859 | — |
Reaction Steps
The distilled oil from Example 3 (1.1 g.) was heated under reflux with 48% hydrobromic acid (10 ml.) for 2 hours. The product was isolated by a procedure analogous to that described in Example 6 to give the title compound (1.07 g.), m.p. 210°-211° C. (Found: C, 58.35; H, 8.0; N, 4.2% C16H25NO HBr requires: C, 58.5; H, 8.0; N, 4.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022764 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-24d8ef5d8a194ff5a43111ebdbe6450a |
| Source note | uspto-grants-1977_05 |