Hydrogen Bromide → HCID 21435859, compound

HRID 2397522Notes

Reaction equation

HRID 2397522 reaction equation
[CH2:1]([C:3]1([C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([O:18]C)[CH:13]=2)[CH2:9][CH2:8][CH:7]([CH3:10])[CH2:6][N:5]([CH3:11])[CH2:4]1)[CH3:2].[BrH:20]>>[BrH:20].[CH2:1]([C:3]1([C:12]2[CH:13]=[C:14]([OH:18])[CH:15]=[CH:16][CH:17]=2)[CH2:9][CH2:8][CH:7]([CH3:10])[CH2:6][N:5]([CH3:11])[CH2:4]1)[CH3:2]

Participants

3

Reactant 2

HCID 260Hydrogen BromideHCID 21435857HCID 21435857, compound

Product 1

HCID 21435859HCID 21435859, compound

Procedure

The distilled oil from Example 3 (1.1 g.) was heated under reflux with 48% hydrobromic acid (10 ml.) for 2 hours. The product was isolated by a procedure analogous to that described in Example 6 to give the title compound (1.07 g.), m.p. 210°-211° C. (Found: C, 58.35; H, 8.0; N, 4.2% C16H25NO HBr requires: C, 58.5; H, 8.0; N, 4.3%).

Workup

  1. customThe product was isolated by a procedure analogous to

Sources & evidence

ORD record
ord-24d8ef5d8a194ff5a43111ebdbe6450a
Source dataset
uspto-grants-1977_05
Patent number
US04022764

Reaction notes

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