HRID2397547

反应详情

EQUATION

反应方程式

HRID 2397547 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Two parts of 6-chloro-2-ethyl-1H-imidazo[4,5-b]quinoxaline was suspended in 40 parts of methanol. One part of concentrated HCl was added to give a solution. A solid formed at once and the slurry was cooled and filtered to give 2 parts of 6-chloro-2-ethyl-1H-imidazo[4,5-b]quinoxaline hydrochloride, m.p. 280°-282°.

WORKUP

后处理

  1. customto give a solution
  2. customA solid formed at once and the slurry
  3. temperaturewas cooled
  4. filtrationfiltered