Acetic Acid → HCID 20313274, compound

Participants

Reaction Steps

To a mixture of 140 grams of 1-Butyl, 2-propyl, 3,5-diethyl 1,2-dihydropyridine and 2-propyl 3,5-diethylpyridine prepared as described in example 1 was added 18 grams of acetic acid, the mixture was stirred for 18 hours at ambient temperature in the presence of air. The resulting reaction product was extracted with water. The water insoluble fraction was identified as 2-propyl 3,5-diethylpyridine. The aqueous extract was evaporated under diminished pressure to yield 71 grams of N-Butyl, 2-propyl, 3,5-diethylpyridinium acetate, nuclear magnetic resonance spectrum, solvent CCl4. δ in ppm, 9.20 m, 1H; 8.33, m, 1H; 4.78 m, 2H; 2.95, m, 6H; 1.80 s, 3H; 1.33, m, and 0.99 m, 18H.

Provenance & Evidence