HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 21436377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 21436379 | HCID 21436379 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21436377 | HCID 21436377 | 86.4% |
Reaction Steps
A mixture of 39 g (0.13 mole) of ethyl 5-(4-nitrophenyl)-2-furimidate hydrochloride and 8.6 g (0.14 mole) of ethylenediamine in 400 ml of absolute ethanol was heated under reflux for 61/2 hr and stood in a refrigerator overnight. The yellow solid was collected by filtration and washed with anhydrous ether to give 33 g (85%) of product, m.p. > 300°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022798 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-fbf779a649924ec999a2b30e21a653c0 |
| Source note | uspto-grants-1977_05 |