HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → HCID 21332364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 2-Pentyloxirane | HCID 92215 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21332364 | HCID 21332364 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-heptene oxide (71.8 g.) and hexamethylenediamine (32 g.) and recrystallization of the resulting product from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxyheptylamine] (I: R= CH3 (CH2)4, R' = H, X= (CH2)6, Z= H) (16.5 g., m.p. 131.2°-134.2° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022833 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-59331d7f75264d17986726ef4ccea230 |
| Source note | uspto-grants-1977_05 |