HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → HCID 21332375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 2-Hexyloxirane | HCID 18126 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21332375 | HCID 21332375 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-octene oxide (42 g.) and hexamethylenediamine (19.05 g.) and recrystallization of the resulting product from methanol gave N,N'-(1,6-hexylene)-bis[2-hydroxyoctylamine] (I: R= CH3 (CH2)5, R' = H, X= (CH2)6, Z= H) (17.2 g., m.p. 124.0°-127.4° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022833 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-bd6a00f7a6694f9783a8ec47b0082aef |
| Source note | uspto-grants-1977_05 |