Ethylenediamine → HCID 21332458, compound

HRID 2397817Notes

Reaction equation

HRID 2397817 reaction equation
[CH2:1]1[O:13][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:14]([NH2:17])[CH2:15][NH2:16]>CO>[CH2:14]([NH:17][CH2:1][CH:2]([OH:13])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:15][NH:16][CH2:1][CH:2]([OH:13])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 178581,2-Epoxydodecane

Product 1

HCID 21332458HCID 21332458, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-dodecene oxide (100 g.) and ethylenediamine (16.3 g.) and recrystallization of part (20 g.) of the resulting product (55.3 g.) from methanol gave N,N'-ethylenebis[2-hydroxydodecylamine] (I: R= CH3 (CH2)9, R' = H, X= (CH2)2, Z= H) (13.4 g., m.p. 137.0°-142.0° C.).

Sources & evidence

ORD record
ord-54630cc2e6bb423dbd0008156b7e6eb8
Source dataset
uspto-grants-1977_05
Patent number
US04022833

Reaction notes

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