HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propane sultone → 3-((1-Methylcyclopentyl)amino)propane-1-sulfonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propane sultone | HCID 14264 | — |
| Reactant | Cyclopentanamine, 1-methyl- | HCID 520998 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 3-((1-Methylcyclopentyl)amino)propane-1-sulfonic acid | HCID 16035847 | — |
Reaction Steps
A solution of 1,3-propanesultone (9.4 g, 75 mmol) in 2-butanone (35 mL) was added dropwise to a the crude solution of 1-methyl-1-cyclopentylamine (mixture of solvent from previous step).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642801B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-66bb6a4238b34d41bba2199ffc7e2a15 |
| Source note | uspto-grants-2014_02 |