HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-Hydroxypyridine → HCID 796646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-Hydroxypyridine | HCID 28114 | — |
| Reactant | HCID 12743422 | HCID 12743422 | — |
| Product | HCID 796646 | HCID 796646 | 79.6% |
Reaction Steps
A mixture of 110.0 g of 2-amino-3-pyridinol and 130.0 g of methyl 2-aminocrotonate are heated at an internal temperature of 110°-115° for approximately 4 hours. The solid product is sublimed in vacuo to give about 140.0 g of product, m.p. 144°-145°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022897 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-fcf980d6119143ada01c1551fabc8388 |
| Source note | uspto-grants-1977_05 |