Butyl isocyanate → 2-Propenoic acid, 2-[[(butylamino)carbonyl]oxy]ethyl ester

HRID 2397960Notes

Reaction equation

HRID 2397960 reaction equation
[CH2:1]([N:5]=[C:6]=[O:7])[CH2:2][CH2:3][CH3:4].[C:8]([O:12][CH2:13][CH2:14][OH:15])(=[O:11])[CH:9]=[CH2:10].COC1C=CC(O)=CC=1>>[C:8]([O:12][CH2:13][CH2:14][O:15][C:6](=[O:7])[NH:5][CH2:1][CH2:2][CH2:3][CH3:4])(=[O:11])[CH:9]=[CH2:10]

Participants

4

Reactant 3

HCID 8110Butyl isocyanateHCID 90154-MethoxyphenolHCID 131652-Hydroxyethyl acrylate

Product 1

HCID 1131592-Propenoic acid, 2-[[(butylamino)carbonyl]oxy]ethyl ester

Procedure

145.3 grams of butyl isocyanate and 180.7 grams of 2-hydroxyethyl acrylate, stabilized with 400 ppm of hydroquinone monomethyl ether, were reacted together for 6 hours at 75° C. to give 1-butane carbamic acid 2-acryloyloxyethyl ester.

Workup

  1. customwere reacted together for 6 hours at 75° C.

Sources & evidence

ORD record
ord-246445da7f0242cd95eb8ddd65e90a62
Source dataset
uspto-grants-1977_05
Patent number
US04023208

Reaction notes

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