HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl isocyanate → 2-Propenoic acid, 2-[[(butylamino)carbonyl]oxy]ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| Product | 2-Propenoic acid, 2-[[(butylamino)carbonyl]oxy]ethyl ester | HCID 113159 | — |
Reaction Steps
145.3 grams of butyl isocyanate and 180.7 grams of 2-hydroxyethyl acrylate, stabilized with 400 ppm of hydroquinone monomethyl ether, were reacted together for 6 hours at 75° C. to give 1-butane carbamic acid 2-acryloyloxyethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04023208 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-246445da7f0242cd95eb8ddd65e90a62 |
| Source note | uspto-grants-1977_05 |